2ZEC
Potent, Nonpeptide Inhibitors of Human Mast Cell Tryptase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1 |
| Spacegroup name | P 41 |
| Unit cell lengths | 82.260, 82.260, 170.650 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.130 - 2.059 |
| Rwork | 0.207 |
| R-free | 0.25600 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.632 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 41.130 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 63811 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
