2ZD9
Structure of a Bacterial Cyclic-Nucleotide Regulated Ion Channel
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Detector technology | CCD |
| Collection date | 2007-01-15 |
| Wavelength(s) | 1.08 |
| Spacegroup name | H 3 |
| Unit cell lengths | 283.287, 283.287, 103.507 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 141.420 - 4.000 |
| R-factor | 0.308 |
| Rwork | 0.307 |
| R-free | 0.33300 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.931 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 141.420 |
| High resolution limit [Å] | 4.000 |
| Number of reflections | 26095 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 298 | PEG2000, pH 6.0, temperature 298K, VAPOR DIFFUSION, SITTING DROP |
