2Z4P
Crystal structure of FFRP-DM1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL24XU |
| Synchrotron site | SPring-8 |
| Beamline | BL24XU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 0.834 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 96.317, 96.317, 95.788 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 25.350 - 1.950 |
| R-factor | 0.189 |
| Rwork | 0.189 |
| R-free | 0.21600 |
| Structure solution method | MIR |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.400 |
| Data reduction software | PROCESS |
| Data scaling software | PROCESS |
| Phasing software | AMoRE |
| Refinement software | CNS (1.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.950 |
| Number of reflections | 35542 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
