2Z0T

Crystal structure of hypothetical protein PH0355

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE BL-5A
Synchrotron site	Photon Factory
Beamline	BL-5A
Temperature [K]	100
Detector technology	CCD
Collection date	2006-06-15
Detector	ADSC QUANTUM 315
Wavelength(s)	0.97926, 0.97947, 0.9600
Spacegroup name	P 1
Unit cell lengths	40.082, 51.336, 66.233
Unit cell angles	108.09, 90.02, 109.31

Refinement procedure

Resolution	25.660 - 1.800
R-factor	0.178
Rwork	0.178
R-free	0.21000
Structure solution method	MAD
RMSD bond length	0.005
RMSD bond angle	1.200
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SOLVE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.860
High resolution limit [Å]	1.800	1.800
Number of reflections	41140
<I/σ(I)>	33.8
Completeness [%]	94.0	90.2
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1
1