2YXW
The deletion mutant of Multicopper Oxidase CueO
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL38B1 |
| Synchrotron site | SPring-8 |
| Beamline | BL38B1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-10-05 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 1 |
| Unit cell lengths | 50.326, 51.573, 86.698 |
| Unit cell angles | 83.77, 90.38, 67.14 |
Refinement procedure
| Resolution | 25.900 - 1.500 |
| R-factor | 0.17901 |
| Rwork | 0.177 |
| R-free | 0.20713 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.486 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 25.940 |
| High resolution limit [Å] | 1.500 |
| Number of reflections | 114961 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 16% PEG 3350, 0.16M Potassium Nitrate, 20% Glycerol, VAPOR DIFFUSION, temperature 293K |
