2YN4
L-2-chlorobutryic acid bound complex L-haloacid dehalogenase from a Rhodobacteraceae family bacterium
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.670, 68.580, 157.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.350 - 1.740 |
R-factor | 0.16438 |
Rwork | 0.162 |
R-free | 0.20268 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2yml |
RMSD bond length | 0.009 |
RMSD bond angle | 1.433 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.000 | 1.790 |
High resolution limit [Å] | 1.740 | 1.740 |
Rmerge | 0.060 | 0.400 |
Number of reflections | 47997 | |
<I/σ(I)> | 14.8 | 2.1 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |