2YMZ
Crystal structure of chicken Galectin 2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1998-05-27 |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 65.853, 90.700, 151.657 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.600 - 1.750 |
| R-factor | 0.19112 |
| Rwork | 0.189 |
| R-free | 0.22692 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1qmj |
| RMSD bond length | 0.019 |
| RMSD bond angle | 2.171 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA (CCP4) |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.600 | 1.840 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Rmerge | 0.040 | 0.470 |
| Number of reflections | 90331 | |
| <I/σ(I)> | 18.94 | 2.15 |
| Completeness [%] | 97.6 | 86.4 |
| Redundancy | 1 | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.8 | 2.0 M AMMONIUM SULPHATE, 1% B-MERCAPTOETHANOL AT PH 4.8 |
