2YGG

Complex of CaMBR and CaM

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X10SA
Synchrotron site	SLS
Beamline	X10SA
Temperature [K]	100
Detector technology	CCD
Collection date	2009-06-25
Detector	ADSC CCD
Spacegroup name	C 1 2 1
Unit cell lengths	200.700, 38.350, 34.100
Unit cell angles	90.00, 91.35, 90.00

Refinement procedure

Resolution	37.668 - 2.227
R-factor	0.1763
Rwork	0.173
R-free	0.23170
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	1.156
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.400
High resolution limit [Å]	2.230	2.230
Rmerge	0.090	0.300
Number of reflections	12449
<I/σ(I)>	16.5	5.9
Completeness [%]	96.0	83.3
Redundancy	12.6	11

Crystallization Conditions

crystal ID	method	pH	temperature	details
1