2YGG
Complex of CaMBR and CaM
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-06-25 |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 200.700, 38.350, 34.100 |
| Unit cell angles | 90.00, 91.35, 90.00 |
Refinement procedure
| Resolution | 37.668 - 2.227 |
| R-factor | 0.1763 |
| Rwork | 0.173 |
| R-free | 0.23170 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.156 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.400 |
| High resolution limit [Å] | 2.230 | 2.230 |
| Rmerge | 0.090 | 0.300 |
| Number of reflections | 12449 | |
| <I/σ(I)> | 16.5 | 5.9 |
| Completeness [%] | 96.0 | 83.3 |
| Redundancy | 12.6 | 11 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
