Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 210 |
| Spacegroup name | P 32 |
| Unit cell lengths | 171.908, 171.908, 454.592 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.992 - 4.500 |
| R-factor | 0.1653 |
| Rwork | 0.167 |
| R-free | 0.23970 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1xck |
| RMSD bond length | 0.029 |
| RMSD bond angle | 2.298 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 4.740 |
| High resolution limit [Å] | 4.500 | 4.500 |
| Rmerge | 0.150 | 0.470 |
| Number of reflections | 87597 | |
| <I/σ(I)> | 6 | 2.3 |
| Completeness [%] | 98.2 | 99.7 |
| Redundancy | 2.9 | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
