2YB6
Native human Rad6
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-06-16 |
| Detector | ADSC QUANTUM 210 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 48.050, 48.050, 124.760 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 32.780 - 1.500 |
| R-factor | 0.16781 |
| Rwork | 0.166 |
| R-free | 0.20538 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ayz |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.409 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0099) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.840 | 1.580 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.090 | 0.430 |
| Number of reflections | 22429 | |
| <I/σ(I)> | 13 | 4 |
| Completeness [%] | 98.1 | 97.2 |
| Redundancy | 5.9 | 6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | pH 5.5 |
