2Y73
THE NATIVE STRUCTURES OF SOLUBLE HUMAN PRIMARY AMINE OXIDASE AOC3
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX II BEAMLINE I711 |
| Synchrotron site | MAX II |
| Beamline | I711 |
| Temperature [K] | 183 |
| Detector technology | CCD |
| Collection date | 2006-06-09 |
| Detector | MARRESEARCH SX-165 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 225.755, 225.755, 216.985 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.931 - 2.600 |
| R-factor | 0.1767 |
| Rwork | 0.175 |
| R-free | 0.21260 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1us1 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.776 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.930 | 2.700 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.010 | 0.050 |
| Number of reflections | 99745 | |
| <I/σ(I)> | 17.5 | 5.1 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 11.8 | 11.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.4 | 0.7 M POTASSIUM/SODIUM TARTRATE, 100 MM IMIDAZOLE PH7.4, 200 MM NACL, 2M SODIUM FORMATE |
