2Y5H
FACTOR XA - CATION INHIBITOR COMPLEX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2010-05-07 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 48.888, 74.644, 77.082 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 41.280 - 1.330 |
| R-factor | 0.14801 |
| Rwork | 0.146 |
| R-free | 0.19036 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2jkh |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.425 |
| Data reduction software | XDS |
| Data scaling software | SADABS |
| Phasing software | CCP4 |
| Refinement software | REFMAC (5.6.0093) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.350 |
| High resolution limit [Å] | 1.330 | 1.330 |
| Rmerge | 0.040 | 0.700 |
| Number of reflections | 64894 | |
| <I/σ(I)> | 11.7 | 1.04 |
| Completeness [%] | 99.0 | 97.8 |
| Redundancy | 3.27 | 3.22 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
