2Y44
Crystal structure of GARP from Trypanosoma congolense
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Spacegroup name | P 1 |
| Unit cell lengths | 36.184, 37.795, 40.680 |
| Unit cell angles | 106.17, 111.75, 99.50 |
Refinement procedure
| Resolution | 34.620 - 1.650 |
| R-factor | 0.20176 |
| Rwork | 0.199 |
| R-free | 0.25085 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.402 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | autoSHARP |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.620 | 1.710 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmerge | 0.090 | 0.450 |
| Number of reflections | 20523 | |
| <I/σ(I)> | 10.9 | 3.5 |
| Completeness [%] | 93.1 | 89 |
| Redundancy | 7.86 | 6.85 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
