Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-03-16 |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.810, 45.810, 45.720 |
| Unit cell angles | 90.00, 103.58, 90.00 |
Refinement procedure
| Resolution | 19.993 - 1.979 |
| R-factor | 0.2031 |
| Rwork | 0.200 |
| R-free | 0.26630 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.149 |
| Data reduction software | MOSFLM |
| Data scaling software | XIA |
| Phasing software | PHASER |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.170 | 2.030 |
| High resolution limit [Å] | 1.980 | 1.980 |
| Rmerge | 0.080 | 0.590 |
| Number of reflections | 12018 | |
| <I/σ(I)> | 10.4 | 2.6 |
| Completeness [%] | 96.8 | 90.9 |
| Redundancy | 3.7 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | 25% PEG-6000, 0.1 M HEPES PH7.0 |
