2XRN

Crystal structure of TtgV

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	C 1 2 1
Unit cell lengths	70.862, 116.184, 71.881
Unit cell angles	90.00, 104.34, 90.00

Refinement procedure

Resolution	44.609 - 2.900
R-factor	0.2156
Rwork	0.212
R-free	0.27900
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.986
Data reduction software	MOSFLM
Phasing software	PHASER
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	69.000
High resolution limit [Å]	2.900
Rmerge	0.080
Number of reflections	12547
Completeness [%]	99.7
Redundancy	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1