2XNC
Crystal structure of an engineered Ferredoxin NADP reductase (FNR) from Pisum sativum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 108 |
Detector technology | IMAGE PLATE |
Collection date | 2008-11-28 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 113.425, 140.259, 51.216 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.040 - 2.900 |
R-factor | 0.198 |
Rwork | 0.197 |
R-free | 0.23500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qg0 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.120 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | BUSTER-TNT (2.8.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.900 | 3.060 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.090 | 0.530 |
Number of reflections | 18774 | |
<I/σ(I)> | 11.7 | 2.9 |
Completeness [%] | 99.7 | 100 |
Redundancy | 4.6 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | pH 8 |