2XL4
LntA, a virulence factor from Listeria monocytogenes
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-09-28 |
Detector | MARRESEARCH |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 49.672, 49.672, 141.799 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.850 - 2.300 |
R-factor | 0.23323 |
Rwork | 0.232 |
R-free | 0.25521 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.020 |
RMSD bond angle | 1.972 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 6.830 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.080 | 0.500 |
Number of reflections | 8491 | |
<I/σ(I)> | 24.9 | 7 |
Completeness [%] | 96.4 | 90.3 |
Redundancy | 13.6 | 13.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.15 M NASO4 18% PEG 3350 |