2XJZ
Crystal structure of the LMO2:LDB1-LID complex, C2 crystal form
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 77 |
| Detector technology | IMAGE PLATE |
| Collection date | 2009-05-15 |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 179.920, 55.530, 114.710 |
| Unit cell angles | 90.00, 90.11, 90.00 |
Refinement procedure
| Resolution | 48.320 - 2.800 |
| R-factor | 0.2289 |
| Rwork | 0.228 |
| R-free | 0.24400 |
| Structure solution method | MAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.130 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | BUSTER (2.9.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.850 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.140 | 0.840 |
| Number of reflections | 27216 | |
| <I/σ(I)> | 18.8 | 1.8 |
| Completeness [%] | 96.7 | 73.2 |
| Redundancy | 7.3 | 6.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5 | 1.6 M NACL, 100 MM MES PH5 AND 1 MM DTT |
