2XJX
Structure of HSP90 with small molecule inhibitor bound
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 44.950, 41.050, 49.230 |
| Unit cell angles | 90.00, 101.86, 90.00 |
Refinement procedure
| Resolution | 43.990 - 1.660 |
| R-factor | 0.1577 |
| Rwork | 0.155 |
| R-free | 0.20760 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.394 |
| Refinement software | BUSTER-TNT (2.5.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 43.990 |
| High resolution limit [Å] | 1.660 |
| Rmerge | 0.060 |
| Number of reflections | 20868 |
| Completeness [%] | 96.6 |
| Redundancy | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
