2XJG

Structure of HSP90 with small molecule inhibitor bound

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Spacegroup name	P 1 21 1
Unit cell lengths	47.200, 41.305, 52.319
Unit cell angles	90.00, 102.71, 90.00

Refinement procedure

Resolution	30.960 - 2.250
R-factor	0.2148
Rwork	0.211
R-free	0.28050
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.012
RMSD bond angle	1.200
Refinement software	BUSTER-TNT (2.5.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.970
High resolution limit [Å]	2.250
Rmerge	0.100
Number of reflections	9503
Completeness [%]	99.7
Redundancy	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1