2XF4

Crystal structure of Salmonella enterica serovar typhimurium YcbL

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	100
Spacegroup name	P 41 21 2
Unit cell lengths	124.363, 124.363, 35.594
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.300
R-factor	0.19471
Rwork	0.193
R-free	0.22896
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.008
RMSD bond angle	1.137
Refinement software	REFMAC (5.5.0047)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.300
Rmerge	0.100
Number of reflections	12665
<I/σ(I)>	46.34
Completeness [%]	96.9
Redundancy	29.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1				0.1M MES, 1.5M SODIUM PHOSPHATE (FINAL PH 6.5)