2XBG
Crystal Structure of YCF48 from Thermosynechococcus elongatus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-01-24 |
| Detector | ADSC CCD |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 55.726, 75.676, 148.549 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 37.838 - 1.500 |
| R-factor | 0.164 |
| Rwork | 0.161 |
| R-free | 0.21640 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.012 |
| RMSD bond angle | 2.226 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHELXCD |
| Refinement software | REFMAC (5.5.0104) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.870 | 1.580 |
| High resolution limit [Å] | 1.400 | 1.500 |
| Rmerge | 0.070 | 0.290 |
| Number of reflections | 50546 | |
| <I/σ(I)> | 5.44 | 1.22 |
| Completeness [%] | 99.8 | 99.9 |
| Redundancy | 4.21 | 3.65 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.1M MAGNESIUM SULFATE, 10% W/V PEG 3350. |
