2X82

Evolutionary basis of HIV restriction by the antiretroviral TRIMCyp

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E SUPERBRIGHT
Temperature [K]	100
Spacegroup name	P 21 21 21
Unit cell lengths	47.470, 116.770, 129.360
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	86.680 - 2.600
R-factor	0.21869
Rwork	0.215
R-free	0.27982
Structure solution method	OTHER
RMSD bond length	0.014
RMSD bond angle	1.536
Refinement software	REFMAC (5.5.0109)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.600
Rmerge	0.100
Number of reflections	22894
<I/σ(I)>	6.6
Completeness [%]	95.7
Redundancy	2.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1