2X2Z

Crystal structure AMA1 from Toxoplasma gondii

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-2
Synchrotron site	SSRL
Beamline	BL9-2
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 1
Unit cell lengths	66.150, 76.070, 88.250
Unit cell angles	72.19, 71.44, 72.90

Refinement procedure

Resolution	43.900 - 2.000
R-factor	0.183
Rwork	0.180
R-free	0.24800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.023
RMSD bond angle	1.932
Refinement software	REFMAC (5.5.0088)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	52.240
High resolution limit [Å]	2.000	2.000
Rmerge	0.070	0.430
Number of reflections	98629
<I/σ(I)>	13.7	3.3
Completeness [%]	96.4	95.3
Redundancy	4	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1