Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 4A |
| Synchrotron site | PAL/PLS |
| Beamline | 4A |
| Temperature [K] | 97 |
| Detector technology | CCD |
| Collection date | 2007-05-15 |
| Detector | ADSC CCD |
| Spacegroup name | P 3 2 1 |
| Unit cell lengths | 121.846, 121.846, 33.575 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 39.880 - 2.300 |
| R-factor | 0.21976 |
| Rwork | 0.219 |
| R-free | 0.23456 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.027 |
| RMSD bond angle | 1.905 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.080 | 0.080 |
| Number of reflections | 13136 | |
| <I/σ(I)> | 32 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 100 | 18.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.1M SODIUM CHLORIDE, 0.1M BIS-TRIS PH6.5, 1.5M AMMONIUM SULFATE |
