2X25
Free acetyl-CypA orthorhombic form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 287 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 42.222, 52.404, 89.236 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.190 - 1.200 |
| R-factor | 0.12756 |
| Rwork | 0.126 |
| R-free | 0.15568 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.033 |
| RMSD bond angle | 2.408 |
| Refinement software | REFMAC (5.5.0088) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 44.000 |
| High resolution limit [Å] | 1.200 |
| Rmerge | 0.090 |
| Number of reflections | 62683 |
| <I/σ(I)> | 5.3 |
| Completeness [%] | 98.5 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
