2WX4
Asymmetric trimer of the Drosophila melanogaster DCP1 C-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-04-12 |
Detector | MARRESEARCH |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 120.920, 120.920, 134.470 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.790 - 2.800 |
R-factor | 0.21725 |
Rwork | 0.215 |
R-free | 0.26675 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2WX3 TRUNCATED POLY-ALA MODEL |
RMSD bond length | 0.011 |
RMSD bond angle | 1.272 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.870 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 14564 | |
<I/σ(I)> | 13 | 2 |
Completeness [%] | 98.2 | 96 |
Redundancy | 4.8 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 100 MM MES (PH6.5), 1.2 M AMMONIUM SULFATE, 5% 1,4-DIOXANE |