2WX1

TAB2 NZF DOMAIN IN COMPLEX WITH Lys63-linked tri-ubiquitin, P212121

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	30.490, 70.920, 72.820
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	32.391 - 3.000
R-factor	0.2251
Rwork	0.222
R-free	0.26910
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.001
RMSD bond angle	0.325
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	70.890
High resolution limit [Å]	3.000
Rmerge	0.120
Number of reflections	3385
<I/σ(I)>	6.9
Completeness [%]	98.6
Redundancy	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1