2WX0

TAB2 NZF DOMAIN IN COMPLEX WITH Lys63-linked di-ubiquitin, P21

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 1 21 1
Unit cell lengths	55.390, 73.620, 59.250
Unit cell angles	90.00, 105.91, 90.00

Refinement procedure

Resolution	38.799 - 2.400
R-factor	0.1769
Rwork	0.174
R-free	0.23590
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.099
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	24.900	2.530
High resolution limit [Å]	2.400	2.400
Rmerge	0.090	0.580
Number of reflections	18032
<I/σ(I)>	10.9	2
Completeness [%]	99.9	99.8
Redundancy	3.4	3.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1