2WWZ

TAB2 NZF DOMAIN IN COMPLEX WITH Lys63-linked di-ubiquitin, P212121

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	30.980, 69.610, 71.520
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	22.193 - 1.400
R-factor	0.1792
Rwork	0.178
R-free	0.20180
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.006
RMSD bond angle	1.082
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	23.400
High resolution limit [Å]	1.400
Rmerge	0.060
Number of reflections	30078
<I/σ(I)>	10.8
Completeness [%]	96.4
Redundancy	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1