2WUX
the crystal structure of recombinant baculovirus polyhedra
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-03-12 |
| Detector | RAYONIX |
| Wavelength(s) | 0.9778, 0.9778 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 102.582, 102.582, 102.582 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.268 - 1.838 |
| R-factor | 0.1663 |
| Rwork | 0.164 |
| R-free | 0.21700 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.042 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SHARP |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.910 |
| High resolution limit [Å] | 1.840 | 1.840 |
| Rmerge | 0.210 | |
| Number of reflections | 15809 | |
| <I/σ(I)> | 12.1 | 1 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 14.7 | 10.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.5 |
