2WUX
the crystal structure of recombinant baculovirus polyhedra
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-12 |
Detector | RAYONIX |
Wavelength(s) | 0.9778, 0.9778 |
Spacegroup name | I 2 3 |
Unit cell lengths | 102.582, 102.582, 102.582 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.268 - 1.838 |
R-factor | 0.1663 |
Rwork | 0.164 |
R-free | 0.21700 |
Structure solution method | SIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 1.042 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.910 |
High resolution limit [Å] | 1.840 | 1.840 |
Rmerge | 0.210 | |
Number of reflections | 15809 | |
<I/σ(I)> | 12.1 | 1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 14.7 | 10.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |