2WUJ
DivIVA N-terminal domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-10-01 |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 29.089, 32.753, 134.542 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 67.200 - 1.400 |
| R-factor | 0.18815 |
| Rwork | 0.186 |
| R-free | 0.22189 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.031 |
| RMSD bond angle | 2.599 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0054) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.000 | 1.480 |
| High resolution limit [Å] | 1.400 | 1.400 |
| Rmerge | 0.070 | 0.140 |
| Number of reflections | 22664 | |
| <I/σ(I)> | 11.2 | 4.8 |
| Completeness [%] | 94.5 | 88.7 |
| Redundancy | 3.3 | 2.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
