Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-12-27 |
| Detector | MARRESEARCH |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 189.948, 189.948, 189.948 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 30.000 - 2.700 |
| R-factor | 0.22228 |
| Rwork | 0.221 |
| R-free | 0.23734 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2bk0 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.217 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 77.600 | 2.850 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 0.090 | 0.400 |
| Number of reflections | 31520 | |
| <I/σ(I)> | 13 | 3.1 |
| Completeness [%] | 96.8 | 96.5 |
| Redundancy | 3.6 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.4 | 2% PEG 400, 100MM NA CITRATE PH 5.4, 2M AMMONIUM SULFATE |
