Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX10.1 |
| Synchrotron site | SRS |
| Beamline | PX10.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-01-27 |
| Detector | MARRESEARCH |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 65.006, 65.006, 239.194 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 36.470 - 1.500 |
| R-factor | 0.15746 |
| Rwork | 0.156 |
| R-free | 0.19085 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1j9l |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.591 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.3.0037) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 36.500 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.080 | 0.190 |
| Number of reflections | 91484 | |
| <I/σ(I)> | 22 | 3 |
| Completeness [%] | 95.9 | 68.2 |
| Redundancy | 8.7 | 2.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 4.5 | 2.5 M NACL, 0.1 M ACETATE PH 4.5, 0.2 M LI SULFATE, OIL (TERA), MICROBATCH UNDER OIL |
