2WOF

EDTA treated E. coli copper amine oxidase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX14.2
Synchrotron site	SRS
Beamline	PX14.2
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 4r
Spacegroup name	P 21 21 21
Unit cell lengths	135.079, 166.880, 79.802
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.960 - 2.250
R-factor	0.16868
Rwork	0.167
R-free	0.22041
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.020
RMSD bond angle	1.704
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.5.0066)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	51.300	2.370
High resolution limit [Å]	2.250	2.250
Rmerge	0.090	0.410
Number of reflections	83024
<I/σ(I)>	13.7	3.9
Completeness [%]	99.9	100
Redundancy	4.4	4.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1