2WO0

EDTA treated E. coli copper amine oxidase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM14
Synchrotron site	ESRF
Beamline	BM14
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	P 21 21 21
Unit cell lengths	134.676, 166.619, 79.834
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.520 - 2.600
R-factor	0.18422
Rwork	0.182
R-free	0.24794
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.014
RMSD bond angle	1.531
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	REFMAC (5.5.0066)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.000	2.740
High resolution limit [Å]	2.600	2.600
Rmerge	0.070	0.240
Number of reflections	56001
<I/σ(I)>	13.2	3.9
Completeness [%]	99.9	99.8
Redundancy	3.6	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1