2WNV

Complex between C1q globular heads and deoxyribose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Collection date	2008-05-15
Detector	ADSC QUANTUM 4
Spacegroup name	P 1
Unit cell lengths	48.350, 48.330, 88.060
Unit cell angles	92.39, 92.60, 113.57

Refinement procedure

Resolution	19.710 - 1.250
R-factor	0.17629
Rwork	0.175
R-free	0.20176
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1pk6
RMSD bond length	0.006
RMSD bond angle	1.095
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.400
High resolution limit [Å]	1.250	1.250
Rmerge	0.060	0.290
Number of reflections	167366
<I/σ(I)>	19.15	5.4
Completeness [%]	83.0	72.1
Redundancy	1.7	1.05

Crystallization Conditions

crystal ID	method	pH	temperature	details
1