2WM3
Crystal structure of NmrA-like family domain containing protein 1 in complex with niflumic acid
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-06-21 |
| Detector | MARRESEARCH |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 68.712, 68.712, 183.789 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.850 |
| R-factor | 0.16734 |
| Rwork | 0.166 |
| R-free | 0.19709 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.017 |
| RMSD bond angle | 2.116 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.5.0089) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.050 | 1.900 |
| High resolution limit [Å] | 1.850 | 1.850 |
| Rmerge | 0.120 | 0.800 |
| Number of reflections | 38676 | |
| <I/σ(I)> | 11.6 | 2 |
| Completeness [%] | 97.8 | 99 |
| Redundancy | 6 | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 2.1M SODIUM MALATE PH 7.0 |
