Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM30A |
| Synchrotron site | ESRF |
| Beamline | BM30A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-11-06 |
| Detector | MARRESEARCH |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 88.990, 88.990, 183.923 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 21.230 - 1.800 |
| R-factor | 0.16302 |
| Rwork | 0.161 |
| R-free | 0.18367 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2bh7 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.403 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 21.380 | 1.900 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.080 | 0.410 |
| Number of reflections | 41725 | |
| <I/σ(I)> | 22.5 | 3.7 |
| Completeness [%] | 98.0 | 99.6 |
| Redundancy | 8.9 | 6.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4 | 1M LICL, 10 % PEG 6K, 0.1M ZNCL2, PH 4 |
