2WJ9
ArdB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF |
| Synchrotron site | ESRF |
| Beamline | ID14-3 |
| Temperature [K] | 100 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 57.900, 67.640, 80.610 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 80.580 - 1.620 |
| R-factor | 0.19264 |
| Rwork | 0.191 |
| R-free | 0.21792 |
| Structure solution method | MIR |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.241 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 23.000 | 1.710 |
| High resolution limit [Å] | 1.620 | 1.620 |
| Rmerge | 0.050 | 0.400 |
| Number of reflections | 36476 | |
| <I/σ(I)> | 13 | 2.8 |
| Completeness [%] | 93.0 | 97 |
| Redundancy | 2.9 | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
