2WJ0
Crystal structures of Holliday junction resolvases from Archaeoglobus fulgidus bound to DNA substrate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-04 |
Detector | MARRESEARCH |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 110.980, 110.980, 150.500 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.056 - 3.100 |
R-factor | 0.2051 |
Rwork | 0.202 |
R-free | 0.27810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wiz |
RMSD bond length | 0.005 |
RMSD bond angle | 1.047 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.180 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.140 | 0.890 |
Number of reflections | 9975 | |
<I/σ(I)> | 15.18 | 2.89 |
Completeness [%] | 95.1 | 86.3 |
Redundancy | 11.86 | 12.41 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 20% W/V PEG 3350, 0.2 M TRI-LITHIUM CITRATE TETRAHYDRATE, 0.01M HEXAAMINE- COBALT(III) CHLORIDE, pH 7.5 |