2WDB
A family 32 carbohydrate-binding module, from the Mu toxin produced by Clostridium perfringens, in complex with beta-D-glcNAc-beta(1,2) mannose
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113.15 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 91.276, 91.276, 132.701 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 79.060 - 2.030 |
| R-factor | 0.19743 |
| Rwork | 0.194 |
| R-free | 0.25958 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.299 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 39.520 |
| High resolution limit [Å] | 2.030 |
| Rmerge | 0.090 |
| Number of reflections | 41797 |
| <I/σ(I)> | 11.6 |
| Completeness [%] | 99.7 |
| Redundancy | 6.97 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
