2WCU
Crystal structure of mammalian FucU
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 297 |
| Spacegroup name | P 1 |
| Unit cell lengths | 38.950, 47.444, 55.550 |
| Unit cell angles | 76.22, 72.25, 81.96 |
Refinement procedure
| Resolution | 20.000 - 1.900 |
| R-factor | 0.19 |
| Rwork | 0.190 |
| R-free | 0.20600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ogd |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.310 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | CCP4 |
| Refinement software | CNS (1.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.970 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.060 | 0.210 |
| Number of reflections | 24544 | |
| <I/σ(I)> | 21.8 | 2.1 |
| Completeness [%] | 85.6 | 53.3 |
| Redundancy | 2.9 | 1.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
