2W8J
SPT with PLP-ser
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 74.248, 108.375, 91.213 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.900 - 1.500 |
R-factor | 0.159 |
Rwork | 0.157 |
R-free | 0.18700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.208 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0070) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 1.540 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.080 | 0.520 |
Number of reflections | 55582 | |
<I/σ(I)> | 8.6 | 1.6 |
Completeness [%] | 99.0 | 89 |
Redundancy | 8 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |