2W82
The structure of ArdA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 63.810, 103.440, 172.980 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.440 - 2.800 |
| R-factor | 0.209 |
| Rwork | 0.207 |
| R-free | 0.24900 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.817 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 12.500 | 2.870 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.064 | 0.565 |
| Number of reflections | 27101 | |
| <I/σ(I)> | 12.6 | 1.8 |
| Completeness [%] | 93.3 | 93.6 |
| Redundancy | 2.5 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
