2W6B
Crystal Structure of the Trimeric beta-PIX Coiled-Coil Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 63 |
Unit cell lengths | 43.120, 43.120, 79.430 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.720 - 2.800 |
R-factor | 0.279 |
Rwork | 0.278 |
R-free | 0.30500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ba2 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.563 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.080 | 0.240 |
Number of reflections | 2079 | |
<I/σ(I)> | 25.7 | 14.5 |
Completeness [%] | 99.5 | 100 |
Redundancy | 21 | 22 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 35% MPD, 0.24 M NON-DETERGENT SULPHOBETAINE 195 (NDSB-195) |