2W67
BtGH84 in complex with FMA34
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-05-09 |
Detector | ADSC CCD |
Spacegroup name | P 1 |
Unit cell lengths | 51.248, 92.101, 98.292 |
Unit cell angles | 103.42, 95.11, 100.60 |
Refinement procedure
Resolution | 87.710 - 2.250 |
R-factor | 0.183 |
Rwork | 0.181 |
R-free | 0.22900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vvn |
RMSD bond length | 0.013 |
RMSD bond angle | 1.465 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.4.0077) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 87.710 | 2.370 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.060 | 0.290 |
Number of reflections | 75364 | |
<I/σ(I)> | 11.2 | 2.5 |
Completeness [%] | 93.3 | 94 |
Redundancy | 2 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.3M NH4AC 10% GLYCEROL 15% PEG3350 0.1M MES PH6 |