2W4S
novel RNA-binding domain in Cryptosporidium parvum at 2.5 angstrom resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-02-17 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.180, 52.862, 99.315 |
Unit cell angles | 90.00, 94.05, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.450 |
R-factor | 0.196 |
Rwork | 0.193 |
R-free | 0.25400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PARTIAL MODEL IN ANOTHER SPACE GROUP |
RMSD bond length | 0.012 |
RMSD bond angle | 1.468 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.580 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.070 | 0.330 |
Number of reflections | 14569 | |
<I/σ(I)> | 7.4 | 2.2 |
Completeness [%] | 94.4 | 73 |
Redundancy | 4.6 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 1.2M NA/K TARTRATE, 100 MM BIS-TRIS PH 5.5 |