2W3Y
Structure of the Evf virulence factor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 69.560, 86.715, 91.457 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 62.870 - 2.000 |
| R-factor | 0.203 |
| Rwork | 0.200 |
| R-free | 0.25000 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.179 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 80.000 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.100 |
| Number of reflections | 38113 |
| <I/σ(I)> | 25.6 |
| Completeness [%] | 100.0 |
| Redundancy | 27.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 25% PEG4000, 50MM BICINE PH 8 |
