2W38
Crystal structure of the pseudaminidase from Pseudomonas aeruginosa
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Spacegroup name | P 21 3 |
| Unit cell lengths | 126.200, 126.200, 126.200 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 33.740 - 1.900 |
| R-factor | 0.176 |
| Rwork | 0.175 |
| R-free | 0.19800 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.474 |
| Data scaling software | SCALA |
| Phasing software | SOLVE |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.040 | 0.310 |
| Number of reflections | 50018 | |
| <I/σ(I)> | 18 | 2.1 |
| Completeness [%] | 95.0 | 70 |
| Redundancy | 2.8 | 1.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
